Microscale and Macroscale Techniques in the Organic Laboratory
by Pavia, Donald L.; Lampman, Gary M.; Kriz, George S.; Engel, Randall G.Edition: 1st
Format: Hardcover
Pub. Date: 2001-08-13
Publisher(s): Cengage Learning
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List Price: $171.12
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Summary
The well-known and tested organic chemistry laboratory techniques of the two best-selling organic chemistry lab manuals: INTRODUCTION TO ORGANIC LABORATORY TECHNIQUES: A SMALL SCALE APPROACH and INTRODUCTION TO ORGANIC LABORATORY TECHNIQUES: A MICROSCALE APPROACH, 3/e are now assembled in one textbook. Professors can use any experiments alongside MICROSCALE AND MACROSCALE TECHNIQUES IN THE ORGANIC LABORATORY. Experiments can be selected and assembled from the two Pavia organic chemistry lab manuals, from professors' homegrown labs, or even competing texts. The 375 page, hardcover book serves as a reference for all students of organic chemistry. With clearly written prose and accurately drawn diagrams, students can feel confident setting up and running organic labs.
Table of Contents
| 1. Laboratory Safety | |
| 2. Advance Preparation and Laboratory Records | |
| 3. Laboratory Glassware | |
| 4. How to Find Data for Your Compound: Handbooks and Catalogues | |
| 5. Measurement of Volume and Weight | |
| 6. Heating and Cooling Methods | |
| 7. Reaction Methods | |
| 8. Filtration | |
| 9. Physical Constants of Solids: The Melting Point | |
| 10. Solubility | |
| 11. Crystallization: Purification of Solids | |
| 12. Extractions, Separations, and Drying Agents | |
| 13. Physical Constants of Liquids: Boiling Point and Density | |
| 14. Simple Distillation | |
| 15. Fractional Distillation; Azeotropes | |
| 16. Vacuum Distillation; Manometers | |
| 17. Sublimation | |
| 18. Steam Distillation | |
| 19. Column Chromatography | |
| 20. Thin-Layer Chromatography | |
| 21. High-Performance Liquid Chromatography (HPLC) | |
| 22. Gas Chromatography | |
| 23. Polarimetry | |
| 24. Refractometry | |
| 25. Infrared Spectroscopy | |
| 26. Nuclear Magnetic Resonance Spectroscopy (Proton NMR) | |
| 27. Carbon-13 Nuclear Magnetic Resonance Spectroscopy | |
| 28. Mass Spectrometry | |
| 29. Computational Chemistry | |
| 30. Guide to the Chemical Literature |
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